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SciX 2026, the annual conference presented by the Federation of Analytical Chemistry and Spectroscopy Societies (FACSS), ran October 4–9, 2026, at the Nugget Casino Resort in Sparks, Nevada. The program spanned atomic and molecular spectroscopy, mass spectrometry, chemometrics, and bioanalysis. This report follows the meeting day by day, from Monday's clinical Raman plenaries to Friday's closing talks, drawing on the online program and Spectroscopy coverage of award winners, highlighting efforts to move Raman, SERS, LIBS, and single-particle ICP-MS toward clinical, environmental, and field use.