Preparing samples for analysis carries a set of difficulties that are often expounded on when cryogenic treatment of the material is necessary to meet the analytical requirements. In order to achieve the application requirements, selection of the correct milling device and technique is a critical decision.
John Philip Walters, Ph.D. (1938-2026), was an analytical chemist who spent 17 years researching the physics of spark-discharge emission spectroscopy at the University of Wisconsin-Madison before moving to St. Olaf College in 1982, where he became best known for pioneering a role-playing undergraduate laboratory model that had students take on professional roles to mirror real analytical-chemistry work. His 1991 three-part series on the approach in Analytical Chemistry earned him the ACS Division of Analytical Chemistry's J. Calvin Giddings Award in 1993, and he continued extending his understand-the-system teaching philosophy into computer-controlled instrumentation well into his later career.
Top content published this week include a new article on bioprocess monitoring, a new “Chemometrics in Spectroscopy” column, and an overview of the latest advancements in laser-induced breakdown spectroscopy (LIBS).