Milestone

This webinar will provide practical guidance regarding sample preparation for ICP-OES and ICP-MS analyses and overcoming the challenges presented by battery-related materials.

https://www.spectroscopyonline.com/spec_w/li-ion

The quality and performance of Li-ion batteries requires elemental analysis of battery components in several steps of the value chain. For example, starting with raw materials, quantitation of the primary elements helps to determine the most appropriate extraction approach. In battery production, it is used to control impurities, as they directly impact the performance and lifespan of the batteries. Elemental analysis is also used during recycling to help purify valuable materials.

Sample preparation is the first fundamental step in ensuring reliable analysis and providing appropriate solutions for both ICP-OES and ICP-MS. Due to the variety of samples and their respective natures, from organic (like graphite) to inorganic (like ores), the sample prep protocol must ensure complete digestion to achieve the high-quality analyses required in this market.
This webinar will address the challenges related to sample preparation by considering several matrices encountered in the Li-ion battery value chain. Practical guidance will be provided for method development by exploring the most critical sample prep factors for ICP-OES and ICP-MS analysis, such as sample mass, temperature, pressure, and acid compatibility. By considering a total-workflow approach to sample prep, additional opportunities for improving lab productivity, quality, and safety will be demonstrated.

The role of sample preparation in elemental analysis of Li-ion battery components

How to address the challenges in sample prep for various matrices

Practical approaches to method development

Key sample prep factors and their impact on ICP-OES and ICP-MS analysis

 is the Product Specialist for the digestion and clean chemistry lines at Milestone, Inc. In 2005m, Eric obtained his bachelor’s degree in Biochemistry from Union College with a focus in Inorganic Chemistry. Prior to joining Milestone, he worked in the particle characterization field as a laboratory manager and in domestic and international sales, where he supported sales and applications across all product lines.



Webcasts

Webinar Date/Time: Wed, May 17, 2023 11:00 AM EDT

Li-ion Batteries: Sample Prep Guidelines for Elemental Analysis

Looking for ways to improve your elemental analysis in areas such as lab throughput, data quality, labor, costs, and safety? This eWorkshop uses a “total workflow” approach to sample preparation that promises to help you optimize your operations and offers practical advice for preventing workflow disruptions that affect your lab’s performance.

https://www.spectroscopyonline.com/spec_w/elemental-analysis

As the performance of atomic spectroscopy techniques for elemental analysis has improved over the past several decades, there has been a concurrent need for improvements in sample preparation. While the sample digestion step appropriately draws the most attention in the preparation process, there are other important steps in the sample preparation workflow that also impact the outcomes of the laboratory, some of which may be unexpected in scope and scale.

This eWorkshop presents a “total workflow” approach to sample preparation and examines ways to improve key aspects of elemental analysis such as lab throughput, data quality, costs, and safety. Just as importantly, it also offers practical advice for preventing workflow disruptions, such as incomplete digestions or sample contamination, which can prevent a laboratory from meeting their overall performance, cost, and safety goals.

Several of the presentations include demonstrations of the systems and methods being discussed, including acid purification, automated reagent addition, vessel handling, microwave digestion, sample filtering, and labware cleaning.



Why you should look beyond sample digestion and consider the total sample preparation workflow for elemental analysis

Approaches for improving your lab’s throughput, quality, flexibility, safety, and costs

Ways to avoid workflow disruptions that have negative effects on your lab’s outcomes

Anyone performing or overseeing elemental analysis

Overview of a “Total Workflow” Approach to Sample Prep and Why it Matters



This introduction of a ‘total workflow’ approach to sample preparation for elemental analysis examines not only the evolution of the pivotal microwave digestion process, but also additional steps in the workflow that are critical to meeting lab performance requirements. By optimizing these steps, laboratories are better prepared to overcome the challenges they face and avoid workflow disruptions that impede the analysis process and can have additional effects.





High-purity acid expenses for elemental analysis labs can consume a significant portion of their operational budgets. In addition, accidental contamination and supply chain challenges for obtaining high-purity acids can put a lab’s operations at risk. In this presentation, you will learn the principles of sub-boiling distillation and how bringing acid purification in-house can result in considerable cost savings and ensure an uninterrupted analysis workflow.






The reagent addition, or “dosing,” step of the sample preparation process has traditionally been a tedious and laborious task within elemental analysis labs, especially when it involves concentrated acids. This presentation shows how automating the reagent dosing process provides greater consistency, while removing the operator from exposure to harmful acid fumes and freeing them to perform safer and more value- added tasks.



Rotor-based Microwave Digestion, Vessel Handling, and Sample Filtering



While still considered the “workhorse” of many elemental analysis laboratories, rotor- based digestion vessels can be cumbersome to handle, and the systems can also be the weak link in a laboratory's sample prep workflow if something goes wrong. In this presentation you will learn how various aspects of rotor-based digestion vessels, systems, and accessories can work to optimize a workflow, as well as avoid disruptions such as the need to rerun samples.



 Single Reaction Chamber Microwave Digestion



The introduction of Single Reaction Chamber (SRC) microwave digestion technology provided a step-change in sample prep performance and capabilities for elemental analysis. In the context of workflow, SRC’s benefits include higher overall sample throughput, faster digestions for difficult samples, and reduced labor requirements. By digesting all samples, regardless of type or acid chemistry, at the same temperature and pressure, it works to avoid incomplete digestions that can lead to mass and optical spectral interferences, sample reruns, and increased instrument downtime.



 Introducing ultraWAVE 3 – Third-generation Benchtop SRC technology



The third generation of benchtop SRC-based instruments has been recently released, providing further benefits to the sample prep workflow for elemental analysis. A redesigned reaction chamber allows a significant increase in the number of samples per digestion run. Innovations such as enhanced automation, increased corrosion resistance, and advanced thermal controls work together to lower the labor requirements, reduce the potential for contamination and operational errors, and increase the number of digestion runs that can be performed both in a single day and over the lifetime of the system.





Using acid baths and microwave systems for cleaning sample prep vessels and other types of labware can have a substantial impact on an elemental analysis lab’s throughput, workflow, and efficiency. In this presentation, you will learn how automating this step using acid-steam cleaning keeps your microwave system focused on digesting samples and removes the tedium and hazards of hand-cleaning labware from your staff.





Multiple scenarios for elemental analysis laboratories are presented, showing how decisions related to sample prep workflow can affect a lab’s performance, costs, and safety.



has been working at Milestone since 2003. He is a chemist and started his career at Milestone as an application specialist, focusing on new method development and addressing specific needs in sample preparation. Later he transitioned to area manager for most countries of Latin America eastern Europe, and the US. Since 2018, he has held the position of marketing manager at Milestone headquarters in Bergamo, Italy. During his career at Milestone, Giulio has worked with hundreds of laboratories and chemists to help them in overcoming daily challenges in elemental analysis by optimizing their workflow and methods. Today, Giulio aims to support worldwide laboratories to enhance their efficiency using state-of-the-art technologies.




Product and Applications Manager
Milestone Inc.



 earned his bachelor’s degree from New Mexico State University and shortly after relocated to Las Vegas, Nevada, to start his career as a chemist in the nutraceutical industry. In this role, he tested incoming raw materials and outgoing finished products using ICP-MS, HPLC, and GC. Once cannabis regulations started coming to fruition in the state, he took a chemist position at a newly licensed lab to help design and implement the facility for Nevada's compliance testing regulations, with a specific focus on heavy metals and microbiology testing. Eventually Stephen moved from the contract lab environment into cannabis production and manufacturing, taking a position as VP of production for Planet 13. In this position, he designed and managed an 18,000-square-foot production facility, formulating over 40 edible SKU's, from carbonated beverages to chocolates and gummies. Stephen is currently the product and applications manager for Milestone Inc., overseeing marketing, research, and customer needs across Milestone’s equipment lines in the US.



 has been an application chemist at Milestone for over 15 years. Thanks to continuous collaboration with laboratories and universities located all over the world, he has gained substantial expertise in sample preparation for elemental analysis over the course of his career. His specialization is in the use of Milestone’s microwave-based instrumentation line that is dedicated to sample digestion, which includes both rotor-based systems and Single Reaction Chamber technology. He is also one of the company’s experts for its Clean Chemistry products that are used to reduce trace element contamination in samples and reagents. In addition to developing new sample prep application methods, Gianpaolo participates in international fairs and conferences, organizes training classes focused on sample preparation, and provides ready support to elemental analysis laboratories.



 is the product specialist for the Digestion and Clean Chemistry lines at Milestone Inc. Eric obtained his bachelor’s degree in biochemistry from Union College in 2005 with a focus in inorganic chemistry. Prior to joining Milestone, he worked in the particle characterization field as a laboratory manager and in domestic and international sales, where he supported sales and applications across all product lines.



Webinar Date/Time: Thu, Apr 27, 2023 11:00 AM EDT


How to Use a “Total Workflow” Sample Prep Approach to Optimize Elemental Analysis

Articles

This application note describes how single reaction chamber (SRC) microwave technology helps prepare challenging materials in Li-ion batteries for elemental analysis.

Milestone

Articles

Li-ion Batteries: Sample Prep Guidelines for Elemental Analysis

How to Use a “Total Workflow” Sample Prep Approach to Optimize Elemental Analysis

Sample Prep for Li-ion Battery Materials

Preparation of Pharmaceutical Samples in Accordance with USP <232>/<233>

Understanding the Advantages of Microwave Extraction Technology for Environmental Labs

Essentials of Elemental Analysis in the Li-ion Battery Chain

Superior Lab Efficiency in Determination of Organic Pollutants in Soil

Application report: Mining ores, catalysts, superalloys, and ceramics

Advanced Microwave Digestion Performance for High-Volume Pharmaceutical Laboratories

Utilizing Direct Mercury Analysis for Mercury Detection in Botanical Extracts, Vitamins and Dietary Supplements