Authors


Craig Jones

Latest:

Rapid Multielement Nanoparticle Analysis Using Single-Particle ICP-MS/MS

Complex isobaric and polyatomic spectral interferences can be mitigated using triple quadrupole ICP-MS (ICP-MS/MS) with a collision–reaction cell (CRC). This configuration allows for the multielement characterization and detection of smaller nanoparticle sizes.


Andrea Raab

Latest:

High Throughput Determination of Inorganic Arsenic in Rice Using Hydride Generation-ICP-MS

A fast and sensitive method using hydride generation (HG) with ICP-MS has been developed for the separation and detection of toxic inorganic arsenic (iAs) in foodstuffs. The iAs measured values in 31 commercial rice products all fell below the current legislative maximum level of 150 µg/kg set by China. Comparing the results obtained by HG-ICP-MS and HPLC-ICP-MS showed comparable limits of detection were achieved.


Jorg Feldmann

Latest:

High Throughput Determination of Inorganic Arsenic in Rice Using Hydride Generation-ICP-MS

A fast and sensitive method using hydride generation (HG) with ICP-MS has been developed for the separation and detection of toxic inorganic arsenic (iAs) in foodstuffs. The iAs measured values in 31 commercial rice products all fell below the current legislative maximum level of 150 µg/kg set by China. Comparing the results obtained by HG-ICP-MS and HPLC-ICP-MS showed comparable limits of detection were achieved.


Helga Gunnlaugsdottir

Latest:

High Throughput Determination of Inorganic Arsenic in Rice Using Hydride Generation-ICP-MS

A fast and sensitive method using hydride generation (HG) with ICP-MS has been developed for the separation and detection of toxic inorganic arsenic (iAs) in foodstuffs. The iAs measured values in 31 commercial rice products all fell below the current legislative maximum level of 150 µg/kg set by China. Comparing the results obtained by HG-ICP-MS and HPLC-ICP-MS showed comparable limits of detection were achieved.


Eva M. Krupp

Latest:

High Throughput Determination of Inorganic Arsenic in Rice Using Hydride Generation-ICP-MS

A fast and sensitive method using hydride generation (HG) with ICP-MS has been developed for the separation and detection of toxic inorganic arsenic (iAs) in foodstuffs. The iAs measured values in 31 commercial rice products all fell below the current legislative maximum level of 150 µg/kg set by China. Comparing the results obtained by HG-ICP-MS and HPLC-ICP-MS showed comparable limits of detection were achieved.


Dharmendra Vummiti

Latest:

Total Metals Analysis of Digested Plant Tissue Using an Agilent 4200 Microwave Plasma-AES

Safe, low cost MP-AES analysis of total metal content of a plant-based reference material following microwave digestion is presented. Elements that are difficult to analyze by FAAS such as B and P were included, with all data acquired in a single run. Accurate determinations over a wide concentration range and with better detection limits and sample throughput compared to FAAS were obtained.


Dorina Magdalena Chipara

Latest:

Raman Spectroscopy of Carbonaceous Materials: A Concise Review

A critical review focused on the Raman spectroscopy of carbonaceous materials and of polymer-based nanocomposites that contain carbonaceous (nano) materials as fillers


Mario Voglino

Latest:

Multi-Residue Pesticide Analysis Using a GC Triple Quadrupole Mass Spectrometer

There are currently more than 1000 pesticides in use worldwide in the production of foodstuffs. There is a significant risk to human health and the environment due to increased pesticide use, poor agricultural practices and illegal use.


Stephanie C. Tucker

Latest:

Agricultural and Environmental Management with Raman Spectroscopy

Raman spectroscopy is applied to quality control of agricultural products with greater frequency, and can also be used to refine regulatory criteria for both agricultural and environmental monitoring. It is now integrated into everything from hand held SERS detectors to unmanned aerial vehicles to monitor the gamut from genetic variation to soil and water content. Development opportunities, particularly with bundled technologies, continue to emerge as demand for quality assurance increases.


Kenneth V. Honn

Latest:

Agricultural and Environmental Management with Raman Spectroscopy

Raman spectroscopy is applied to quality control of agricultural products with greater frequency, and can also be used to refine regulatory criteria for both agricultural and environmental monitoring. It is now integrated into everything from hand held SERS detectors to unmanned aerial vehicles to monitor the gamut from genetic variation to soil and water content. Development opportunities, particularly with bundled technologies, continue to emerge as demand for quality assurance increases.


Rachel E. Kast

Latest:

Agricultural and Environmental Management with Raman Spectroscopy

Raman spectroscopy is applied to quality control of agricultural products with greater frequency, and can also be used to refine regulatory criteria for both agricultural and environmental monitoring. It is now integrated into everything from hand held SERS detectors to unmanned aerial vehicles to monitor the gamut from genetic variation to soil and water content. Development opportunities, particularly with bundled technologies, continue to emerge as demand for quality assurance increases.


Tayro E. Acosta

Latest:

Detection of Chemicals with Standoff Raman Spectroscopy

A compact standoff Raman system can be used to detect hazardous chemicals and chemicals used in homemade explosives synthesis.


L.K.H. Bittner

Latest:

Using Near-Infrared Spectroscopy to Monitor the Curing Reaction of Silicone Adhesives

In recent years there has been increased use of silicones in medicine, especially for medicinal implants. Quality control of intracorporeal-used silicones is an important task for ensuring patients’ health, but it is also a challenging one. The traditional mechanical methods used for the quality control of these silicone products, like rheometric measurements, tend to waste a lot of raw material. In this study, near-infrared spectroscopy (NIRS) has been used to replace the traditional method (rheometric measurements of control samples) using rheometry only as reference method to generate different calibration models. The applicability of NIRS as non-invasive analysis method is proven and the developed calibration models for curing processes of a silicone-adhesive at different temperatures are shown.


John A. McLean

Latest:

Advanced Structural Mass Spectrometry for Systems Biology: Pulling the Needles from Haystacks

Ion mobility–mass spectrometry (IM-MS) is outlined as a separations method, several examples of the utility of IM-MS for complex biological measurements are illustrated, and the implications of this approach for systems biology research are discussed.


Matthew Nigro

Latest:

High Temperature and Pressure Automated Sequential Microwave Digestion of Bunker Oil

CEM's Discover SP-D Gold microwave digestion system with high temperature and pressure chamber enables safe, fast, and automated preparation of previously difficult sample types



Vincenzo Palleschi

Latest:

Avoiding Misunderstanding Self-Absorption in Laser-Induced Breakdown Spectroscopy (LIBS) Analysis

The physics and chemistry of the phenomenon have been well known for many years, and this knowledge can tell us how self-absorption can be not only “corrected,” but also tuned to our advantage in analytical applications of LIBS.


Stefano Legnaioli

Latest:

Applying LIBS to Metals Processing

The monitoring of the processes in steel and metal industry calls for techniques that are capable of measuring the composition of metallic alloys at a distance and on moving conveyor belts. In many cases, such as in the recycling of automotive scrap, the geometry of the objects to be analyzed can vary, and surface coatings can be present. In this paper, we discuss the application of LIBS to two industrial projects to illustrate how the above-mentioned problems can be faced and successfully resolved.


Giulia Lorenzetti

Latest:

Applying LIBS to Metals Processing

The monitoring of the processes in steel and metal industry calls for techniques that are capable of measuring the composition of metallic alloys at a distance and on moving conveyor belts. In many cases, such as in the recycling of automotive scrap, the geometry of the objects to be analyzed can vary, and surface coatings can be present. In this paper, we discuss the application of LIBS to two industrial projects to illustrate how the above-mentioned problems can be faced and successfully resolved.


Emanuela Grifoni

Latest:

Applying LIBS to Metals Processing

The monitoring of the processes in steel and metal industry calls for techniques that are capable of measuring the composition of metallic alloys at a distance and on moving conveyor belts. In many cases, such as in the recycling of automotive scrap, the geometry of the objects to be analyzed can vary, and surface coatings can be present. In this paper, we discuss the application of LIBS to two industrial projects to illustrate how the above-mentioned problems can be faced and successfully resolved.


Stefano Pagnotta

Latest:

Applying LIBS to Metals Processing

The monitoring of the processes in steel and metal industry calls for techniques that are capable of measuring the composition of metallic alloys at a distance and on moving conveyor belts. In many cases, such as in the recycling of automotive scrap, the geometry of the objects to be analyzed can vary, and surface coatings can be present. In this paper, we discuss the application of LIBS to two industrial projects to illustrate how the above-mentioned problems can be faced and successfully resolved.


Audrey L. Ingram

Latest:

VT-DRIFTS Investigations of Interactions Between Benzoic Acid and Montmorillonite Clay

High stability Fourier transform-infrared (FT-IR) interferometers make it possible to conduct experiments designed to identify subtle sample structure changes resulting from external perturbations. In particular, IR spectrum measurements obtained while heating samples can be used to associate specific structure changes with incremental additions of thermal energy. This paper describes the application of variable temperature diffuse reflection infrared Fourier transform spectroscopy (VT-DRIFTS) for analysis of benzoic acid adsorbed on montmorillonite clay. The technique described here is generally applicable for soil adsorbate characterization studies, and therefore should be useful for elucidating soil transport mechanisms for selected contaminants.


Tara M. Nickels

Latest:

VT-DRIFTS Investigations of Interactions Between Benzoic Acid and Montmorillonite Clay

High stability Fourier transform-infrared (FT-IR) interferometers make it possible to conduct experiments designed to identify subtle sample structure changes resulting from external perturbations. In particular, IR spectrum measurements obtained while heating samples can be used to associate specific structure changes with incremental additions of thermal energy. This paper describes the application of variable temperature diffuse reflection infrared Fourier transform spectroscopy (VT-DRIFTS) for analysis of benzoic acid adsorbed on montmorillonite clay. The technique described here is generally applicable for soil adsorbate characterization studies, and therefore should be useful for elucidating soil transport mechanisms for selected contaminants.


Dalia K. Maraoulaite

Latest:

VT-DRIFTS Investigations of Interactions Between Benzoic Acid and Montmorillonite Clay

High stability Fourier transform-infrared (FT-IR) interferometers make it possible to conduct experiments designed to identify subtle sample structure changes resulting from external perturbations. In particular, IR spectrum measurements obtained while heating samples can be used to associate specific structure changes with incremental additions of thermal energy. This paper describes the application of variable temperature diffuse reflection infrared Fourier transform spectroscopy (VT-DRIFTS) for analysis of benzoic acid adsorbed on montmorillonite clay. The technique described here is generally applicable for soil adsorbate characterization studies, and therefore should be useful for elucidating soil transport mechanisms for selected contaminants.


Robert L. White

Latest:

VT-DRIFTS Investigations of Interactions Between Benzoic Acid and Montmorillonite Clay

High stability Fourier transform-infrared (FT-IR) interferometers make it possible to conduct experiments designed to identify subtle sample structure changes resulting from external perturbations. In particular, IR spectrum measurements obtained while heating samples can be used to associate specific structure changes with incremental additions of thermal energy. This paper describes the application of variable temperature diffuse reflection infrared Fourier transform spectroscopy (VT-DRIFTS) for analysis of benzoic acid adsorbed on montmorillonite clay. The technique described here is generally applicable for soil adsorbate characterization studies, and therefore should be useful for elucidating soil transport mechanisms for selected contaminants.


Zacariah L. Hildenbrand

Latest:

Analytical Efforts Toward Monitoring Groundwater in Regions of Unconventional Oil and Gas Exploration

A mix of analytical methods is required to understand the impact, if any, that UOG activity is having on groundwater.


Robin L. Pulliam

Latest:

Fourier-Transform Molecular Rotational Resonance Spectroscopy: Bridging the Gap Between Spectroscopy and Chromatography for VOC Analysis

This study demonstrates the strengths of FT-MMR for simple, direct analysis of VOCs and other toxic industrial chemicals.


Justin L. Neill

Latest:

Fourier-Transform Molecular Rotational Resonance Spectroscopy: Bridging the Gap Between Spectroscopy and Chromatography for VOC Analysis

This study demonstrates the strengths of FT-MMR for simple, direct analysis of VOCs and other toxic industrial chemicals.


Matthew T. Muckle

Latest:

Fourier-Transform Molecular Rotational Resonance Spectroscopy: Bridging the Gap Between Spectroscopy and Chromatography for VOC Analysis

This study demonstrates the strengths of FT-MMR for simple, direct analysis of VOCs and other toxic industrial chemicals.


Brent H. Harris

Latest:

Fourier-Transform Molecular Rotational Resonance Spectroscopy: Bridging the Gap Between Spectroscopy and Chromatography for VOC Analysis

This study demonstrates the strengths of FT-MMR for simple, direct analysis of VOCs and other toxic industrial chemicals.