July 4th 2025
This study used three distinct sample preparation techniques to examine the metal content of geological rocks.
Application of SERS to the Determination of Butylated Hydroxyanisole in Edible and Essential Oils
July 1st 2015Surface-enhanced Raman scattering (SERS) has been applied to the determination of the antioxidant butylated hydroxyanisole (BHA), commonly used in fatty foods and oils to prevent their oxidation. The use of SERS-Raman microscopy with an inexpensive homemade silver substrate allowed the direct determination of BHA in oils without any sample handling. Several edible and essential oils (used as flavorings) have been considered for this purpose.
A method for the multielemental determination of metals and nonmetals in goji berries (Lycium barbarum L.) by axially and radially viewed inductively coupled plasma-optical emission spectrometry (ICP-OES) is presented.
Sequentially Shifted Excitation Raman Spectroscopy
November 1st 2014A method for removing fluorescence-induced backgrounds from Raman spectra using sequentially shifted excitation (SSE) is described. The method uses a temperature-tuned, distributed Bragg reflector diode laser to produce the multiple excitation spectra required to implement the SSE algorithm. Examples applying the SSE method to analysis of motor oils and edible oils are given.
Macro ATR-FT-IR Spectroscopic Imaging of Dynamic Processes
October 1st 2014Macro attenuated total reflection FT-IR spectroscopic imaging is a powerful and underutilized tool. This article presents an overview of approaches and opportunities for using this method to study dynamic processes such as diffusion, sorption, crystallization, and dissolution.
How Trace Elemental Analysis Provides Important Insight into Wine Chemistry
September 1st 2014Examples are shown that highlight how elemental fingerprinting could provide valuable information about the geographical origin of a food or beverage as well as how different steps in the production of wines impact their elemental composition.
Rapid Determination of Trace Metals in Oil Using Handheld X-Ray Fluorescence Spectroscopy
July 1st 2014Determination of trace metals in oil and petroleum typically is based on ICP-OES methods, requiring signficant sample preparation and expensive instrumentation. This article presents an alternative method, based on the use of a handheld energy-dispersive X-ray fluorescence analyzer, that involves minimal sample preparation, uses authentic standards for calibration, gives low parts-per-million detection limits, and provides significant time and cost savings.
Label-Free Chemical Detection in Micro-Fabricated Devices Using FT-IR Spectroscopic Imaging
October 1st 2012Fourier transform infrared (FT-IR) spectroscopic imaging is a highly versatile technique that can be applied to a wide range of systems. This article summarizes some of the recent efforts developing applications of FT-IR imaging for microfluidics. The main advantage of FT-IR imaging compared to traditional imaging methods is that it is a label-free imaging technique.
Label-Free Chemical Detection in Micro-Fabricated Devices Using FT-IR Spectroscopic Imaging
October 1st 2012Fourier transform infrared (FT-IR) spectroscopic imaging is a highly versatile technique that can be applied to a wide range of systems. This article summarizes some of the recent efforts developing applications of FT-IR imaging for microfluidics. The main advantage of FT-IR imaging compared to traditional imaging methods is that it is a label-free imaging technique.