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Latest:
Porous Chitosan Composite Membrane Tandem Laser-Induced Breakdown Spectroscopy for Detection of Metal Elements in Liquid SamplesDetecting metal elements in liquid samples cannot be done efficiently by only using LIBS, but when the technique is combined with appropriate membrane materials, rapid analysis of solution samples can be realized.
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Study on Estimating Total Nitrogen Content in Sugar Beet Leaves Under Drip Irrigation Based on Vis-NIR Hyperspectral Data and Chlorophyll ContentThe relationship between leaf nitrogen content (LNC) and hyperspectral remote sensing imagery (HYP) was determined to construct an estimation model of the LNC of drip-irrigated sugar beets, to enable real-time monitoring of sugar beet growth and nitrogen management in arid areas.
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Extractable and Leachable Testing for Pharmaceutical Packaging, Finished Pharmaceutical Products, and Medical Devices: An Analytical PerspectiveExtractable and leachable (E&L) testing for finished pharmaceutical products, bioprocess manufacturing systems, and medical devices is currently a subject of intense interest. The majority of the challenges encountered in analytical workflows are related to the highly complex matrices and relatively low analyte evaluation thresholds seen in E&L studies. This paper provide options for executing E&L testing to supporting regulatory submissions. There are multiple compliant routes possible, and the presented workflows and analytical solutions are only one of multiple successful approaches.
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Raman Spectroscopy as a Tool for Rapid Feedback of Perovskite Growth Crystallinity and CompositionPerovskites are known to be useful for fabrication of solar cells, and their crystalline structure plays an important role in their electronic properties. Here, we show how Raman analysis is able to confirm the presence of the required crystalline phase for solar cell production.
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Quantifying Ethanol Concentration in Hand Sanitizer via AutomationThe concentration of ethanol in hand sanitizer was determined using a calibration developed with an automated ATR sampling accessory.
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Multiscale Convolutional Neural Network of Raman Spectra of Human Serum for Hepatitis B Disease DiagnosisA multiscale convolutional neural network (MsCNN) was used to screen Raman spectra of the hepatitis B serum, achieving higher classification accuracy compared to traditional machine learning methods.
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Best of the Week: Big Pharma Restructuring, Raman Spectroscopy, Artificial IntelligenceHere are the top five articles that the editors of Spectroscopy published this week.
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Novel LC–MS/MS Method with a Dual ESI and APCI Ion Source for Analysis of California-Regulated Pesticides and Mycotoxins in Medium-Chain Triglyceride (MCT) Oil Cannabis TincturesAnalysis of 66 pesticides and 5 mycotoxins regulated by the State of California in cannabis tinctures were analyzed using LC–MS/MS with an ESI source, and LC–MS/MS with an APCI source. A simple, fast, and cheap acetonitrile solvent extraction method was used for sample preparation for good recovery and high throughput, and internal standards were used to compensate for ion suppression effects from the hydrophobic matrix.
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In situ Raman Spectroscopy Monitors the Corrosion of Mild Steel in a Salt Fog ChamberIn this study, in situ Raman spectroscopy was used to detect the formation, growth, and evolution of corrosion inside a salt fog chamber. These results pave the way for monitoring the real-time observation of corrosion on metal surfaces.
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Investigating a Laser-Induced Titanium Plasma Under an Applied Static Electric FieldWe investigate the effect of an applied electric field on the laser-induced titanium plasma for laser induced breakdown spectroscopy (LIBS) for the purpose of assessing electron density with respect to laser energy.
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Manipulating Sound with Lasers and OpticsLasers are used for a wide range of industrial, medical, spectroscopic, and military applications. Daniel Kazal, a graduate research assistant in the Department of Chemistry and Biochemistry at the University of Maryland Baltimore County, has developed a novel technique for channeling sound using a tube-shaped laser beam that forms a thermal gradient. Based on his work with this approach, he received the 2017 FACSS Innovation Award. We recently spoke with him about this research. This interview is part of a series of interviews with the winners of awards presented at SciX.
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Real-World Application of Open-Path UV-DOAS, TDL, and FT-IR Spectroscopy for Air Quality Monitoring at Industrial FacilitiesThe implementation of 120 open-path spectroscopy analyzers at oil refineries has taught us lessons about compound identification, target species detectability, interferences, and data management, which can help spectroscopists generate more accurate data when monitoring air quality.
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Fluorescence Quenching Effects of Fe3+ Ions on Carbon DotsThe “selective fluorescence quenching effects” of Fe3+ ions on carbon dots are examined to gain a more comprehensive understanding of the interactions of metal ions with a variety of fluorescent materials.
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Raman Spectroscopy in BioprocessingExamining Raman spectroscopy use with a Raman Rxn2 analyzer with a Rxn-10 probe and bIO-Optic for monitoring and controlling parameters in upstream bioprocessing.
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Towards Automated Routine Analysis of the Distribution of Trace Elements in Single Cells Using ICP-MSAnalysis of the compositional variation in living cells is essential for understanding biological processes. Single-cell elemental analysis by triple-quadrupole ICP-MS is emerging as a selective, highly sensitive, and potentially high-throughput technique for the study of constitutive elements, and uptake of metallodrugs (or metal-containing nanomaterials) in single cells.
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Exploring the Potential of the Yb(III) (HE)4 Complex for Oncotherapy Using UV-vis SpectroscopyEvaluation of the UV-vis spectra of the reaction product of ytterbium (III) with hematoxylin (HE) indicates the formation of a rare earth complex that further reacts with marine mammal DNA, indicating the potential that this complex may have anti-tumor properties.
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Fluorescence Quenching Effects of Fe3+ Ions on Carbon DotsThe “selective fluorescence quenching effects” of Fe3+ ions on carbon dots are examined to gain a more comprehensive understanding of the interactions of metal ions with a variety of fluorescent materials.
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Energy Dispersive XRF in Soil Analysis for the Agrifood SectorIn the agrifood sector, soil sampling and analysis is a prerequisite for accurate fertilizer management and to monitor the accumulation of heavy metals in soils. In this study, energy dispersive X-ray fluorescence (EDXRF) was used to analyze soils with variable textures (clay and sandy) and the percent recovery of elements was compared, as a measure of accuracy.
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Measurement of Ammonia Leakage by TDLAS in Mid-Infrared Combined with an EMD-SG Filter MethodIn this article, tunable diode laser absorption spectroscopy (TDLAS) is used to measure ammonia leakage, where a new denoising method combining empirical mode decomposition with the Savitzky-Golay smoothing algorithm (EMD-SG) is proposed to improve the signal-to-noise ratio (SNR) of absorbance signals.
Latest:
Extractable and Leachable Testing for Pharmaceutical Packaging, Finished Pharmaceutical Products, and Medical Devices: An Analytical PerspectiveExtractable and leachable (E&L) testing for finished pharmaceutical products, bioprocess manufacturing systems, and medical devices is currently a subject of intense interest. The majority of the challenges encountered in analytical workflows are related to the highly complex matrices and relatively low analyte evaluation thresholds seen in E&L studies. This paper provide options for executing E&L testing to supporting regulatory submissions. There are multiple compliant routes possible, and the presented workflows and analytical solutions are only one of multiple successful approaches.
Latest:
Preparation and Spectral Properties of MgAl2O4: Tb3+ PhosphorA look at how the spectral properties single-phase green emission phosphor make it suitable for near-UV light-emitting diode (NUV-LED) applications.
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Optical Properties of the Suwannee River Fulvic Acid Complexation with Thorium Using 3D Fluorescence SpectroscopyThe relationship between the complexation amount of thorium (Th) and Suwannee River fulvic acid (SRFA) and the changes in Th concentration and pH were studied using differential spectroscopy and 3D excitation-emission matrix fluorescence spectroscopy (3D EEM).
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Imaging of Trace Elements Using Laser Ablation–Inductively Coupled Plasma–Mass Spectrometry: Emerging New ApplicationsMetallomics seeks to understand the metallobiochemistry of cells and organisms in health and disease. This article explains the principle of laser ablation–inductively coupled plasma–mass spectrometry (LA-ICP-MS) for imaging applications and highlights its potential to provide additional insights in bioanalysis and metallomics.
Latest:
Porous Chitosan Composite Membrane Tandem Laser-Induced Breakdown Spectroscopy for Detection of Metal Elements in Liquid SamplesDetecting metal elements in liquid samples cannot be done efficiently by only using LIBS, but when the technique is combined with appropriate membrane materials, rapid analysis of solution samples can be realized.
Latest:
Investigating a Laser-Induced Titanium Plasma Under an Applied Static Electric FieldWe investigate the effect of an applied electric field on the laser-induced titanium plasma for laser induced breakdown spectroscopy (LIBS) for the purpose of assessing electron density with respect to laser energy.
Latest:
Beyond the Beaker: How to Advance Your Scientific CareerDr. Jeanita Pritchett offers insight on how science, technology, engineering, and math (STEM) students can transition into a successful scientific career after graduation.
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Efficient Discrimination of Some Moss Species by Fourier Transform Infrared Spectroscopy and ChemometricsIn combination with attenuated total reflectance (ATR), Fourier transform infrared (FT-IR) spectroscopy can be used to classify different moss species.
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Review and Prospect: Applications of Exponential Signals with Machine Learning in Nuclear Magnetic ResonanceA review of exponential signal models with machine learning in nuclear magnetic resonance (NMR) spectroscopy is discussed here.
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Efficient Discrimination of Some Moss Species by Fourier Transform Infrared Spectroscopy and ChemometricsIn combination with attenuated total reflectance (ATR), Fourier transform infrared (FT-IR) spectroscopy can be used to classify different moss species.
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EDX and LIBS Studies on Gallstones Using Partial Least Squares Discriminant Analysis (PLS-DA)Understanding gallstone formation requires examining their elemental composition. Here, EDS and LIBS were used with PLS-DA to quantify elements found in human gallstones.
