Near Infrared (NIR) Spectroscopy

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Thomas Mayerhöfer and Jürgen Popp

In this tutorial, Thomas G. Mayerhöfer and Jürgen Popp introduce complex-valued chemometrics as a more physically grounded alternative to traditional intensity-based spectroscopy measurement methods. By incorporating both the real and imaginary parts of the complex refractive index of a sample, this approach preserves phase information and improves linearity with sample analyte concentration. The result is more robust and interpretable multivariate models, especially in systems affected by nonlinear effects or strong solvent and analyte interactions.

Manufactured parts of the 3D printer are printed with metals from powder © OlegDoroshin -chronicles-stock.adobe.com

Researchers at Wroclaw University of Science and Technology and Université catholique de Louvain have demonstrated how diffuse reflectance spectroscopy (DRS) in the 900 nm to 1100 nm range can non-destructively assess powder blend homogeneity in metal additive manufacturing. Their findings suggest that DRS offers a fast, reliable method for ensuring uniformity in aluminum alloy powders used in powder bed fusion 3D printing.

Chemical vapor deposition (CVD) machine creating an optically thin film coating © Your Hand Please-chronicles-stock.adobe.com

Researchers from Northwestern University, University of Cádiz, and University of Arizona have developed new formulae for analyzing optical thin films that outperform traditional models by accounting for complex geometries and absorbing substrates. These advances offer more precise ultraviolet-visible-near-infrared (UV-vis-NIR) spectroscopic analysis of film materials used in critical modern technologies.

Bruce R. Kowalski

In this Icons of Spectroscopy article, Executive Editor Jerome Workman Jr. delves into the life and impact of Bruce Kowalski, an analytical chemist whose major contributions to chemometrics helped establish the field of applying advanced quantitative and qualitative mathematics to extract meaningful chemical information from complex datasets. Kowalski’s visionary approach to chemical data analysis, education, and software development has transformed the landscape of modern analytical chemistry for academia and industry.

Wireless fNIRS sensor concept wearable headband that monitors brain activity in real time © stefanholm-chronicles-stock.adobe.com

Researchers have developed a wireless, wearable brain-monitoring device using functional near-infrared spectroscopy (fNIRS) to detect cognitive fatigue in real time. The miniaturized system enables mobile brain activity tracking, with potential applications in driving, military, and high-stress work environments.