Infrared (IR) Spectroscopy

A new study led by Gaëlle Belleau-Magnat at Université de Sherbrooke reveals that Arctic gossans, analyzed using rover-compatible techniques, may serve as valuable analogs for Martian environments and help guide the search for past life on Mars.

Mississippi State University researchers show that mid-infrared (MIR), a.k.a. infrared (IR), portable spectrometers, combined with calibration transfer techniques, can match lab instruments for soil property analysis.

Researchers at China Agricultural University developed a rapid and accurate spectroscopic method using NIR and FT-IR combined with PLS regression to measure protein content in rice noodles, enhancing quality control for the popular river snail rice noodle (luosifen) industry.

Spectroscopy's 2025 Emerging Leader in Molecular Spectroscopy is Lingyan Shi of the University of California, San Diego. Shi’s research focuses on developing and applying molecular imaging tools, including stimulated Raman scattering (SRS), multiphoton fluorescence (MPF), fluorescence lifetime imaging (FLIM), and second harmonic generation (SHG) microscopy.

This tutorial addresses the critical issue of analyte specificity in multivariate spectroscopy using the concept of Net Analyte Signal (NAS). NAS allows chemometricians to isolate the portion of the signal that is unique to the analyte of interest, thereby enhancing model interpretability and robustness in the presence of interfering species. While this tutorial introduces the foundational concepts for beginners, it also includes selected advanced topics to bridge toward expert-level applications and future research. The tutorial covers the mathematical foundation of NAS, its application in regression models like partial least squares (PLS), and emerging methods to optimize specificity and variable selection. Applications in pharmaceuticals, clinical diagnostics, and industrial process control are also discussed.

A new review article highlights the role Fourier transform infrared (FT-IR) spectroscopy plays in characterizing nanomaterials and polymers.

Researchers at the University of Belgrade have demonstrated that combining Raman and FT-IR spectroscopy with machine learning algorithms offers a highly accurate, non-destructive method for identifying seed varieties in lettuce, paprika, and tomato.

DOGE-related federal funding cuts have sharply reduced salaries, lab budgets, and graduate support in academia. Researchers view the politically driven shifts in priorities as part of recurring systemic issues in U.S. science funding during administrative transitions. The impact on Federal laboratories has varied, with some seeing immediate effects and others experiencing more gradual effects. In general, there is rising uncertainty over future appropriations. Sustainable recovery may require structural reforms, leaner administration, and stronger industry-academia collaboration. New commentary underscores similar challenges, noting scaled-back graduate admissions, spending freezes, and a pervasive sense of overwhelming stress among faculty, students, and staff. This article addresses these issues for the analytical chemistry community.

Top articles published this week include an interview series with Robert Ewing of the Pacific Northwest National Laboratory, a news article on using infrared (IR) cameras to see invisible methane leaks, and an article about the role of vibrational spectroscopy in analyzing plant-based food products.

Researchers in Scotland have developed a drone-mounted infrared imaging system that can detect and map methane gas leaks in real time from up to 13.6 meters away. The innovative approach combines laser spectroscopy with infrared imaging, offering a safer and more efficient tool for monitoring pipeline leaks and greenhouse gas emissions.

Researchers from institutions in Brazil harness near-infrared spectroscopy and machine learning to determine cocoa content with precision.

A new review highlights how vibrational spectroscopy techniques like FTIR, NIR, and Raman offer rapid, non-destructive tools for accurately analyzing plant-based protein content and structure.

Researchers at Xi’an Jiaotong University have demonstrated that ATR-FTIR spectroscopy, combined with histological analysis and machine learning, can accurately distinguish between drowning and strangulation in forensic cases.

A new review led by researchers from MIT and Oak Ridge National Laboratory outlines how artificial intelligence (AI) is transforming the study of molecular vibrations and phonons, making spectroscopic analysis faster, more accurate, and more accessible.

A recent study reports high-purity blue emission and thermal stability in novel lanthanum (III) complex synthesized via low-energy precipitation method.

This tutorial examines the modeling of diffuse reflectance (DR) in complex particulate samples, such as powders and granular solids. Traditional theoretical frameworks like empirical absorbance, Kubelka-Munk, radiative transfer theory (RTT), and the Hapke model are presented in standard and matrix notation where applicable. Their advantages and limitations are highlighted, particularly for heterogeneous particle size distributions and real-world variations in the optical properties of particulate samples. Hybrid and emerging computational strategies, including Monte Carlo methods, full-wave numerical solvers, and machine learning (ML) models, are evaluated for their potential to produce more generalizable prediction models.

Earlier this month, ABB and Hydrosat announced an expansion of their partnership by launching the second infrared (IR) camera that will go aboard Hydrosat’s VanZyl-2 satellite, which is scheduled for summer 2025.

A team of researchers from Spanish institutions has found that polystyrene used in healthcare packaging shows strong resistance to UVC sterilization, with minimal chemical degradation detected using FT-IR and Raman spectroscopy.

The recipient of the 2025 NYSAS Gold Medal Award is Geraldine L. Richmond, Presidential Chair in Science and Professor of Chemistry at the University of Oregon.

Researchers from Ca’ Foscari University of Venice and the University of Padua have uncovered the earliest direct evidence of Upper Palaeolithic humans deliberately processing the non-edible plant Isatis tinctoria, revealing complex behaviors involving medicinal or dye-related plant use over 32,000 years ago.

Fourier transform infrared (FT-IR) spectroscopy was used in this paper to rapidly analyze seven light alkanes (methane, ethane, propane, n-butane, i-butane, n-pentane, and i-pentane) in wellhead gases.

In this tutorial, Thomas G. Mayerhöfer and Jürgen Popp introduce complex-valued chemometrics as a more physically grounded alternative to traditional intensity-based spectroscopy measurement methods. By incorporating both the real and imaginary parts of the complex refractive index of a sample, this approach preserves phase information and improves linearity with sample analyte concentration. The result is more robust and interpretable multivariate models, especially in systems affected by nonlinear effects or strong solvent and analyte interactions.

A recent study published in the journal Food Chemistry explored Brazil’s cachaça industry, focusing on a new analytical method that can confirm the geographic origin of cachaças from the Brejo Paraibano region in Brazil.

Explore advancements in infrared spectroscopy and insights from Brian Smith, a key columnist, on the future of this evolving field.

In Part III, our discussion with Pooja Sheevam focused on the use of long-wave IR (LWIR) spectroscopy in analyzing basaltic rocks.