Application Notes: Atomic Spectroscopy

Miniature X-ray sources reached the development level that is appropriate for their use in the handheld and portable X-Ray diffraction (XRD) instruments. This note describes the application of X-ray sources for the residual stress measurements using XRD.

Spectrochemical analysis is a comparative technique; therefore, unknown samples are best analyzed against reference materials of similar composition.

Miniature X-ray sources reached the development level that is appropriate for their use in the hand held and portable X-Ray diffraction (XRD) instruments. This note describes the application of X-ray sources for the residual stress measurements using XRD.

Data for a handheld LIBS device (SciAps Z-500) is presented demonstrating in-field measurement of several elements critical for geochemical applications. In some cases these elements have never before been measured with a handheld device.

CEM's Discover SP-D Gold microwave digestion system with high temperature and pressure chamber enables safe, fast, and automated preparation of previously difficult sample types

The 12 W miniature source has a higher voltage and a much higher emission current than our present miniature X-ray sources, which is an advantage for a number of applications.

The majority of environmental laboratories are currently using traditional techniques like cold vapor atomic absorption to analyze samples for mercury content.

The TSI® LIBS Desktop Analyzer laser induced breakdown spectroscopy (LIBS) instrument allows simultaneous determination of all detectable elements present in the material being analyzed.

Inks and pigments with optically unique properties can provide quick visual verification of authenticity, and can be difficult to replicate.

In the agri-food sector it is important to not only study the soil composition and use of fertilizers, but also the uptake of nutrients and potentially toxic elements within the plants and crops themselves.

Elemental ratio determinations in foraminiferal calcite require the measurement of trace levels of Na, Mg, Sr, and ultra-trace levels of Li, B, Ba, Cd, Mn, U in a calcium rich matrix and ratioed to calcium.

In gemology the TSI ChemReveal LIBS Desktop Analyzer has been used to aid gemologists in gemstone classification. This paper highlights study results of this instrument in some of those applications.

Peak emission for silicon occurs at values beyond the range of sensitivity for silicon-based detectors, like CCDs. EMCCDs combine a larger field of view and higher resolution with high sensitivity in the NIR at lower cost.

The new Savillex PFA Cyclonic Spray Chamber is the first inert chamber with the traditional shape of a glass cyclonic, and is also the first translucent inert chamber.

Ancient Roman builders designed maritime concrete harbor structures to remain intact in the aggressive seawater environment for very long periods of time.

Milestone's UltraWAVE microwave digestion system with single reaction chamber (SRC) technology, enables the simultaneous digestion of up of to 22 different sample types and chemistries at temperatures and pressures as high as 300 ?C and 199 bar.

The permitted sulfur limit in fuel oils has been decreased to 10 ppm in many regions.

The lanthanide series is a series of metallic elements, with atomic numbers 58 through 71, which are - in order of increasing atomic number - cerium, praseodymium, neodymium, promethium, samarium, europium, gadolinium, terbium, dysprosium, holmium, erbium, thulium, ytterbium, and lutetium.

The new Savillex C400d PFA concentric nebulizer for ICP-MS combines the reliability of a low flow glass nebulizer with the chemical resistance and low elemental background of a PFA concentric nebulizer.

Sample matrices with high organic content have created a significant challenge for sample preparation methods.

This application note introduces an Application Package for quantitative analysis of additive elements in polymer.

This application note describes the capability of the Teledyne Leeman Lab's Prodigy7 High-Dispersion ICP for performing analysis according to SW-846 Method 6010C.

Moxtek now has a full energy dispersive X-ray fluorescence detector solution with Moxtek's XPIN detectors and our new MXDPP-50 electronics.

Demonstration of the advantages of using the Orbis micro-XRF elemental analyzer rather than other analysis techniques to perform elemental analysis through a plastic barrier and/or at atmospheric pressure.

SciAps has developed a handheld analyzer based on laser induced breakdown spectroscopy (LIBS).

With over 1300 commercial testing labs in the United States, one out of every three samples is for water analysis. There has been an even stronger emphasis on mercury testing and its concentration in our water supplies.

Mercury is a toxic, persistent pollutant found in many native ores rich in copper, silver and gold. As such ores are processed mercury can be released to the environment.

Single reaction chamber microwave digestion enables a chemist to digest up to 15 different specialty chemical samples simultaneously at temperatures as high as 300 ?C, greatly simplifying the workflow while maintaining superior quality digestions.

The analysis of coal is demonstrated, with specific emphasis on the measurement of Na2O, using a Cartesian geometry energy dispersive X-ray fluorescence (EDXRF) spectrometer employing the Fundamental Parameters (FP) approach.